Modified electrode for electrochemical analysis.

The electrochemical sensor for As(III) were developed by using carbon nanotube/amino acid modified platinum electrode using cyclic voltammetry. Experimental conditions such as pH, supporting electrolyte and scan rate were optimized. It was observed that the modified electrode has significantly super...

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Main Authors: Yusof, Nor Azah, Daud, Nurulhaidah
Format: Patent
Published: 2009
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id oai:psasir.upm.edu.my:27669
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spelling oai:psasir.upm.edu.my:27669 http://psasir.upm.edu.my/id/eprint/27669/ Modified electrode for electrochemical analysis. Yusof, Nor Azah Daud, Nurulhaidah The electrochemical sensor for As(III) were developed by using carbon nanotube/amino acid modified platinum electrode using cyclic voltammetry. Experimental conditions such as pH, supporting electrolyte and scan rate were optimized. It was observed that the modified electrode has significantly superior analytical performance in determination as As(III) compared to the unmodified electrode. The determination of As(III) by using modified electrode was reproducible with R.S.D of 7.33%. Determination of As(III) was observed to be free interference at pH 4 acetate buffer. The electrocatalytic redox peak current of As(III) showed a linear response towards different concentration of As(III) and linear calibration cuves were obtained. The sensitivity expressed as the slope of the linear regon of the calibration curve. This method was also examined for determination of As(III) in some real samples, such as industrial waste water from wood industry and electroplating industry. 2009-07-07 Patent NonPeerReviewed Nor Azah Yusof (2009) Modified electrode for electrochemical analysis. UNSPECIFIED.
institution UPM IR
collection UPM IR
description The electrochemical sensor for As(III) were developed by using carbon nanotube/amino acid modified platinum electrode using cyclic voltammetry. Experimental conditions such as pH, supporting electrolyte and scan rate were optimized. It was observed that the modified electrode has significantly superior analytical performance in determination as As(III) compared to the unmodified electrode. The determination of As(III) by using modified electrode was reproducible with R.S.D of 7.33%. Determination of As(III) was observed to be free interference at pH 4 acetate buffer. The electrocatalytic redox peak current of As(III) showed a linear response towards different concentration of As(III) and linear calibration cuves were obtained. The sensitivity expressed as the slope of the linear regon of the calibration curve. This method was also examined for determination of As(III) in some real samples, such as industrial waste water from wood industry and electroplating industry.
format Patent
author Yusof, Nor Azah
Daud, Nurulhaidah
spellingShingle Yusof, Nor Azah
Daud, Nurulhaidah
Modified electrode for electrochemical analysis.
author_facet Yusof, Nor Azah
Daud, Nurulhaidah
author_sort Yusof, Nor Azah
title Modified electrode for electrochemical analysis.
title_short Modified electrode for electrochemical analysis.
title_full Modified electrode for electrochemical analysis.
title_fullStr Modified electrode for electrochemical analysis.
title_full_unstemmed Modified electrode for electrochemical analysis.
title_sort modified electrode for electrochemical analysis.
publishDate 2009
_version_ 1819295057062133760
score 13.4562235